分析化学双语实验2025|PDF|Epub|mobi|kindle电子书版本百度云盘下载

分析化学双语实验PDF格式电子书版下载

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第一部分 分析化学实验基本知识1

第二部分 基础实验5

实验一 滴定分析基本操作5

Experiment 1 The Basic Operation in TitrimetricAnalysis9

实验二 电子天平与称量练习14

Experiment 2 Electronic Analytical Balance and Weighing Exercise16

实验三0.1 mol/LHCl标准溶液的配制和标定18

Experiment 3 Preparation and Standardization of Standard 0.1 mol/L Hydrochloric Acid Solution20

实验四 混合碱的含量测定22

Experiment 4 Determination ofMixed Base24

实验五0.1 mol/L氢氧化钠标准溶液的配制与标定26

Experiment 5 Preparation and Standardization of Standard Solution of 0.1 mol/L SodiumHydroxide Solution28

实验六阿司匹林的含量测定30

Experiment 6 Determination ofAspirin32

实验七0.05 mol/LEDTA标准溶液的配制与标定34

Experiment 7 Preparation and Standardization of 0.05 mol/L EDTA Standard Solution36

实验八EDTA对铅、铋混合溶液的连续滴定38

Experiment 8 Continuous Titration ofPb2＋and Bi3＋Mixed Solution by EDTA40

实验九EDTA标准溶液的标定及自来水总硬度的测定42

Experiment 9 EDTA Solution Calibration and Determination of Tap Water Hardness44

实验十0.1 mol/LNa2S2O3标准溶液的配制和标定46

Experiment 10 Preparation and Standardization of 0.1 mol/L Sodium Thiosulfate Standard Solution48

实验十一碘量法测定维生素C的含量51

Experiment 11 VitaminCDeterminationbyIodineTitration53

实验十二碘量法测定葡萄糖的含量55

Experiment 12 Determination ofGlucose by Iodimetry57

实验十三0.02 mol/L高锰酸钾标准溶液的配制与标定59

Experiment 13 Preparation and Standardization of 0.02 mol/L Standard Potassium Permanganate Solution61

实验十四过氧化氢的含量测定63

Experiment 14 Determination ofHydrogen Peroxide65

实验十五硝酸银标准溶液的配制和标定67

Experiment 15 Preparationand Standardizationofthe StandardSilverNitrateSolutions69

实验十六氯化铵的含量测定72

Expenment 16 Determination ofAmmoniumChloride74

实验十七 自来水中氯含量的测定76

Experiment 17 TheDeterminationoftheContentofChlorineinTapWater78

实验十八氯化钡中结晶水测定80

Experiment 18 Determination of Water in Barium Chloride Dihydrate82

实验十九磷酸的电位滴定84

Experiment 19 The Potentiometric Titration of Phosphoric Acid86

实验二十用氟离子选择电极测定水中氟离子含量88

Experiment 20 Determination of F-in Water by Fluorine Ion-Selective Electrode90

实验二十一永停滴定法标定I2标准溶液93

Experiment 21 Standardization of I2Standard Solution by Dead-stop Titration Method95

实验二十二紫外－可见分光光度法测定维生素B12注射液的含量97

Experiment 22 Determination of Vitamin B 12 Injection by UV Spectrophotometry99

实验二十三比色法测定芦丁的含量101

Experiment 23 Determination ofthe Content ofRutin by Colorimetry103

实验二十四荧光分光光度法测定维生素B2的含量105

Experiment 24 Determination ofVitamin B2 by Fluorescence Spectrometry107

实验二十五苯和二甲苯气相色谱实验条件的考察109

Experiment 25 Experimental Conditions Study for Benzene and Methylbenzene AnalyzedbyGas Chromatography111

实验二十六HPLC法测定感冒胶囊中咖啡因的含量114

Experiment 26 Determination ofCaffeine in Ganmao Capsule by HPLC116

实验二十七水杨酸红外光谱的测定118

Experiment 27 Determination of Salicylic Acid Chemical Structure by IR Spectrophotometry120

实验二十八薄层色谱的制备和应用122

Experiment28 Preparation andApplicationofThinLayerChromatography124

第三部分 设计性实验127

实验二十九食醋总酸度的测定127

Experiment29 Determination ofTotalAcidityofVinegar128

实验三十蛋壳中钙、镁的含量测定129

Experiment 30 Determination of Calcium and Magnesium Content in Eggshell130

第四部分 大型分析仪器仿真操作132

实验三十一气相色谱－质谱联用仪的仿真操作132

Experiment 31 Gas ChromatographyMass Spectrometry （GC-MS）134

实验三十二红外光谱仪仿真操作136

Experiment 32 Infrared Spectroscopy（IR）137

实验三十三原子吸收分光光度计的仿真操作139

Experiment 33 Atomic Absorption Spectrophotometer（AAS）142

实验三十四高效液相色谱的仿真操作146

Experiment 34 HighPerformanceLiquidChromatography（HPLC）147

第五部分 附录149

附录1常用指示剂149

附录2常用缓冲溶液的配制152

附录3 0～95 ℃时标准缓冲溶液的pH153

附录4常用酸碱的密度、含量和浓度154

参考文献155